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Type: Artigo de periódico
Title: A new method for the selective quantitation of cyanogenic glycosides by membrane introduction mass spectrometry
Author: Moraes, LAB
Eberlin, MN
Cagnon, JR
Urbano, LH
Abstract: A new method is described for the rapid, sensitive, virtually interference-free, and selective quantitation of cyanogenic glycosides in aqueous extracts using membrane introduction mass spectrometry (MIMS). Selective monitoring, by either conventional MIMS or cryotrap-MIMS, not of HCN but of the co-released ketones (acetone and butan-2-one), when performed for both the crude cassava extracts and the linamarase-NaOH-hydrolyzed extracts, is found to offer an advantageous alternative to classic spectrophotometric methods based on HCN analysis for the selective quantitation of the two cyanogenic glycosides linamarin and lotaustralin expressed as both the free HCN content and the total cyanogenic potential (total HCN).
Country: Inglaterra
Editor: Royal Soc Chemistry
Citation: Analyst. Royal Soc Chemistry, v. 125, n. 9, n. 1529, n. 1531, 2000.
Rights: aberto
Identifier DOI: 10.1039/b004300l
Date Issue: 2000
Appears in Collections:Unicamp - Artigos e Outros Documentos

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