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Type: Artigo de periódico
Title: High-performance liquid chromatographic stationary phases based on poly(dimethylsiloxane) immobilized on silica
Author: Tonhi, E
Collins, KE
Collins, CH
Abstract: This work describes the preparation and characterization of six stationary phases for high-performance liquid chromatography (HPLC) obtained by deposition of poly(dimethylsiloxane) (PDMS). in HPLC silica particles, followed by immobilization using different processes (thermal treatments, thermal treatment + microwave irradiation, self-immobilization + gamma irradiation and self-immobilization + microwave irradiation). The chromatographic parameters of all the phases were evaluated with a mixture of test compounds having varied natures (acid, basic and neutral). The stability of one of these phases was evaluated in both a neutral mobile phase and a higher pH mobile phase used at an elevated temperature, with promising results. © 2005 Elsevier B.V. All rights reserved.
Subject: reversed phase
Country: Holanda
Editor: Elsevier Science Bv
Citation: Journal Of Chromatography A. Elsevier Science Bv, v. 1075, n. 41671, n. 87, n. 94, 2005.
Rights: fechado
Identifier DOI: 10.1016/j.chroma.2005.03.110
Date Issue: 2005
Appears in Collections:Unicamp - Artigos e Outros Documentos

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