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Type: Artigo de periódico
Title: Determination of water content in Brazilian honeybee-collected pollen by Karl Fischer titration
Author: Morgano, MA
Milani, RF
Martins, MCT
Rodriguez-Amaya, DB
Abstract: This paper assesses the performance of a chemical method based on the Karl Fischer titration to determine the water content in samples of dehydrated honeybee-collected pollen. The following analysis parameters were investigated: extraction temperature, particle size, reaction time, and weight of a dried pollen sample. After optimization, the method was used to determine the water content of 154 samples of dried honeybee-collected pollen from different geographical regions of Brazil. The Karl Fischer titration method, performed using a solvent mixture of methanol and n-octanol (1:1 v/v) at 50 degrees C on pollen particles 600 mu m in size produced the best results. Mean values for water content of the 154 samples of dried honeybee-collected pollen from 12 Brazilian regions ranged from 3% to 9%. (C) 2011 Elsevier Ltd. All rights reserved.
Subject: Bee pollen
Water content
Karl Fischer titration
Country: Inglaterra
Editor: Elsevier Sci Ltd
Rights: fechado
Identifier DOI: 10.1016/j.foodcont.2011.03.016
Date Issue: 2011
Appears in Collections:Unicamp - Artigos e Outros Documentos

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