Please use this identifier to cite or link to this item: http://repositorio.unicamp.br/jspui/handle/REPOSIP/56830
Type: Artigo de periódico
Title: Microstructural and electrical properties of PbTIO3 screen-printed thick films
Author: Fechine, PBA
da Rocha, MJS
Santos, MRP
Pereira, FMM
de Menezes, AS
Almeida, JMA
Goes, JC
Ayala, AP
Sombra, ASB
Abstract: In this article we will study the structural and electrical properties of PbTiO3 (PTO) screen-printed thick films. These properties can change with synthetic routes employed for synthesis of PTO. The ceramic powder has been synthesized by mechanical alloying and solid state route. This material crystallizes in the tetragonal system, with space group P4mm and unit cell dimensions a = b = 3.904, c = 4.152 angstrom, and Z = 1. From our results, it was observed that PTO obtained by mechanical alloying provides smaller crystallite size. The Rietveld refinement showed that the samples synthesized by mechanical alloying and solid state route crystallize in the tetragonal system but with different cell parameters. The Raman shifts of these films agree with modes from literature. However, some displacements happen, because the morphology and structural characteristics of the thick films are different, compared to single crystal and thin film. The photomicrographs of the PTO thick films showed that the choice of synthetic routes obtained samples with different microstructures.
Country: Holanda
Editor: Springer
Rights: fechado
Identifier DOI: 10.1007/s10854-007-9429-8
Date Issue: 2008
Appears in Collections:Artigos e Materiais de Revistas Científicas - Unicamp

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