Please use this identifier to cite or link to this item: http://repositorio.unicamp.br/jspui/handle/REPOSIP/55205
Type: Artigo de periódico
Title: Automated flow analysis system based on multicommutation for Cd, Ni and Pb on-line pre-concentration in a cationic exchange resin with determination by inductively coupled plasma atomic emission spectrometry
Author: Miranda, CES
Reis, BF
Baccan, N
Packer, AP
Gine, MF
Abstract: A flow system for on-line pre-concentration of Cd, Ni and Pb and determination by inductively coupled plasma atomic emission spectrometry is presented. The manifold comprised a set of three-way solenoid valves, which were controlled by a microcomputer running software written in Quick Basic 4.5 by means of an A/D board. Since the flow network was based on the multicommutation concept pre-concentration and elution steps could be simultaneously performed in several columns in parallel with significant analytical throughput improvement. Comparing obtained results with certified values, no significant difference at 95% confidence level was observed. Other valuable features such as an analytical throughput of 90 determinations per hour, relative standard deviation <4% (n = 10), sample consumption of 7.8 ml per determination were also achieved. (C) 2002 Elsevier Science B.V. All rights reserved.
Subject: automatization
multicommutation
pre-concentration
ICP-AES
Country: Holanda
Editor: Elsevier Science Bv
Rights: fechado
Identifier DOI: 10.1016/S0003-2670(01)01212-0
Date Issue: 2002
Appears in Collections:Artigos e Materiais de Revistas Científicas - Unicamp

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