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Type: | Artigo |
Title: | Separation and purification of fructooligosaccharides on a zeolite fixed‐bed column |
Author: | Kuhn, Raquel Cristine Mazutti, Marcio Antonio Maugeri Filho, Francisco |
Abstract: | Fructooligosaccharides (FOS), a well-known prebiotic product, are obtained by enzymatic synthesis and consist of a mixture of mono- and disaccharides. In this work, a methodology for their separation and purification was developed using a zeolite fixed-bed column. The effects of column temperature (40-60°C), eluent flow rate (0.10-0.14 mL/min), injected to bed volume percent ratio (2.6-5.1%), and ethanol concentration in the eluent (40-60%, v/v) were investigated using a fractionary factorial design (24-1), having the separation efficiency and purity as target responses. Additional experiments were performed as well, where the temperature and ethanol concentration were studied in a central composite design (22). In this work, the zeolite fixed-bed column was shown to be a good alternative for FOS purification, allowing a FOS purity of 90% and separation efficiency of 6.86 between FOS and glucose, using an eluent at 45°C with 60% ethanol concentration |
Subject: | Zeolitos |
Country: | Alemanha |
Editor: | Wiley |
Rights: | Fechado |
Identifier DOI: | 10.1002/jssc.201300979 |
Address: | https://onlinelibrary.wiley.com/doi/full/10.1002/jssc.201300979 |
Date Issue: | 2014 |
Appears in Collections: | FEA - Artigos e Outros Documentos |
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