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Type: Artigo de evento
Title: New Generation Of Sterically Protected C18 Stationary Phases Containing Embedded Urea Groups For Use In High-performance Liquid Chromatography
Author: Silva C.R.
Jardim I.C.S.F.
Airoldi C.
Abstract: New monofunctional C18 urea stationary phases with sterically protecting dimethyl and diisopropyl groups were prepared by a single step modification process. ProntoSil spherical silica (3 μm) was chemically modified with the monofunctional ethoxysilanes, [(3-octadecylurea)propyl]dimethyl and [(3-octadecylurea)propyl]diisopropyl ethoxysilanes. The phases were characterized by elemental analysis, infrared and solid-state 29Si and 13C NMR spectroscopies. Chromatographic characterizations of the new phases in 50×3.9 mm HPLC columns were performed by the separation of two different test mixtures, containing nonpolar, polar and highly basic compounds. © 2002 Elsevier Science B.V. All rights reserved.
Rights: fechado
Identifier DOI: 10.1016/S0021-9673(02)01807-1
Date Issue: 2003
Appears in Collections:Unicamp - Artigos e Outros Documentos

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