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Type: Artigo de periódico
Title: A high-throughput method for determining chloramphenicol residues in poultry, egg, shrimp, fish, swine and bovine using LC-ESI-MS/MS
Author: Siqueira, SRR
Donato, JL
de Nucci, G
Reyes, FGR
Abstract: A LC-ESI-MS/MS method for determining chloramphenicol residues in fish, shrimp, poultry, eggs, bovine and swine was developed and validated. The samples were extracted with a phosphate extraction solution followed by liquid-liquid extraction with ethyl acetate. The LC was performed on a C18 column at room temperature. For all the matrices, the analytical curves showed r values and recoveries higher than 0.99 and 50%, respectively. The accuracy values lay between 85 and 120% and the precision was lower than 20%. The LOQ was 0.1 ng/g. The method was employed to analyze samples collected in Brazil.
Subject: Bovine
Country: Alemanha
Editor: Wiley-v C H Verlag Gmbh
Citation: Journal Of Separation Science. Wiley-v C H Verlag Gmbh, v. 32, n. 23-24, n. 4012, n. 4019, 2009.
Rights: fechado
Identifier DOI: 10.1002/jssc.200900345
Date Issue: 2009
Appears in Collections:Unicamp - Artigos e Outros Documentos

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